Abstract

Significance The scanning surface inspection system（ SSIS） for wafer surface is an essential tool for quality control in semiconductor manufacturing processes， and its performance evaluation requires calibration using standard wafer （SW） materials. To achieve independent calibration， there is an urgent need for China to develop SW materials that meet calibration requirements.This will address the low domestic production rate of SSIS equipment and further advance the research and application of wafer standard materials in China.

Methods In this paper， a generation-deposition system for SW preparation was developed. The system utilized a differential mobility classifier （DMC） to screen polystyrene aerosols of the desired particle size and a scanning mobility particle sizer （SMPS） to analyze particle size distribution. Through theoretical and experimental analysis， the physical parameters of the deposition chamber were optimized and validated through numerical simulations in Ansys Fluent. Moreover， the influence of operational parameters on uniform deposition and deposition efficiency was investigated.

Conclusions and Prospects When the particle size ranged from 100 to 300 nm， uniform physical parameters of the deposition chamber could achieve similar deposition results. However， for particles with sizes between 40 and 70 nm， different combinations of deposition chamber parameters were required. Deposition uniformity was influenced by the relative rotation position. Under the same conditions， particle size monodispersity was negatively correlated with the flow-to-time ratio. Increasing the deposition time improved deposition efficiency but had no impact on particle size monodispersity. Thermophoretic effect improved deposition efficiency but caused contamination， rendering the contaminated SW unsuitable for SSIS calibration. Rotation increased the deposition spot area by 26% and decreased the concentration by 10%， reducing deposition efficiency but facilitating better control of deposition time and improving distribution uniformity. Differences in particle size distribution between SSIS and SMPS were observed due to their distinct calibration principles.

Conclusion Based on the simulation and experimental results，a 2-inch wafer standard with 200 nm polystyrene particles was successfully prepared， meeting the calibration requirements. The wafer standard materials prepared using this generationdeposition system have traceable particle sizes and a quantity distribution that meets the calibration requirements of the SSIS.

Keywords： aerosol particle； wafer deposition； standard material； numerical simulation

Get Citation: ZHANG Ziheng， REN Jun， LIU Yue2，et al. Method for uniform deposition of polystyrene particles on wafer surface［J］. China.Powder Science and Technology， 2025， 31（6）： 1−14.

DOI：10.13732/j.issn.1008-5548.2025.06.003

Received: 2025-01-16 .Revised: 2024-03-11 ,Online: 2025-05-27

Funding Project: 国家重点研发项目，编号：2023YFF0616400。

First Author: 张子恒（1998—），男，硕士生，研究方向为晶圆标准物质的制备。E-mail：zhangziheng68@163. com。

Corresponding Author:刘俊杰（1975—），男，副研究员，硕士，硕士生导师，研究方向为颗粒物测量及计量技术。E-mail：liujj@nim. ac. cn；

任军（1974—），男，教授，博士生导师，山西高校优秀青年学术带头人、“131”领军人才工程优秀中青年拔尖创新人才，“三晋英才”支持计划拔尖骨干人才、 山西省学术技术带头人，研究方向为碳化学与化工。E-mail：renjun@tyut. edu. cn。

DOI：10.13732/j.issn.1008-5548.2025.06.003

CLC No: TB9； TB4          Type Code: A

Serial No: 1008-5548（2025）06-0001-14