WANG Jianronga,SHI Jieb,GUAN Fangb,HOU Pengkunb
(a.School of Materials Science and Engineering;b.Shandong Provincial Key Lab for the Preparation and Measurement of Building Materials,University of Jinan,Jinan 250022,China)
Abstract:Due to the particle agglomeration phenomenon of nano-SiO2,the particle size distribution and dispersion of nano-SiO2 powder in cement liquid phase were studied by means of LS13320 laser particle size,SEM and TEM.Nano-SiO2 powder was dispersed by ultrasonic pulse technology and the optimal ultrasonic power was determined.The effect of surfactant addition sequence on the particle size distribution of nano-SiO2 in cement liquid phase was studied.The results show that the synergistic effect of ultrasonic pulse and surfactant is the best dispersion method of nano-SiO2.The experimental conditions for obtaining the optimal nano-SiO2 particle size distribution are 5 min ultrasonic time and 360 W ultrasonic power.Surfactant is added to the cement liquid phase after the addition of nano-SiO2,which is more conducive to the dispersion of nano-SiO2.
Keywords:nano-SiO2; cement liquid phase; dispersion; ultrasonic pulse; surfactant
中图分类号:TQ172.1+6
文献标志码:A
文章编号:1008-5548(2021)01-0090-07
DOI:10.13732/j.issn.1008-5548.2021.01.011
收稿日期:2020-06-27,修回日期:2020-09-21,在线出版时间:2020-11-02 10:36。
基金项目:国家自然科学基金项目,编号:51672107;山东省科技重大专项(新兴产业)项目,编号:2015ZDXX0702B01。
第一作者简介:王建荣(1966—),女,学士,高级实验师,研究方向为粉体合成与应用研究。E-mail:mse_wangjr@ujn.edu.cn。