ISSN 1008-5548

CN 37-1316/TU

Journal Online  2018 Vol.24
<Go BackNo.3

Preparation of ultrafine lithium iron phosphate powder by airflow crushing and drying

ZHANG Mingyu1a, LIU Tingnan1b, HUANG Shenglong1b, LYU Juan2 , CHEN Haiyan1b

(1. a. School of Civil Engineering and Architecture; b. School of Environment and Resource, Southwest University of Science and Technology, Mianyang 621000, China; 2.Mianyang Liuneng Powder Equipment Co.,Ltd., Mianyang 621000, China)

Abstract:According to the moisture absorption of ultrafine lithium iron phosphate powder and its crushing requirements, the LNJST-120 HT closed-cycle airflow grinding and grading system with nitrogen gas protection were applied to the superfine processing and drying of the lithium iron phosphate powder. The operating parameters and equipment structure in the system of grinding, grading, collecting, packaging and transporting were analyzed and improved. Meanwhile, the liquidity and moisture content of the powder in the running process were also studied.Through the industrial test of processing ultrafine lithium iron phosphate powder, investigation on the improved supersonic jet milling was adopted. The results show that, when the rotational speed of the screw feeding machine and the classifier are 62 and 1 072 r/m in respectively, the air pressure and temperature are 0.5 MPa and 120 ℃, and the dew point of the packing room is controlled below-20 ℃, the moisture content of lithium iron phosphate powder is maintained from 0.35 ‰ to 0.55 ‰, the mean particle size (d50) is 0.81.2 μm, the maximum particle size (d100) is smaller than 8 μm, and the powder yield is 200~230 kg/h.

Keywords:closed system; supersonic jet milling; lithium iron phosphate powder

中图分类号:TQ110.6            文献标志码:A

文章编号:1008-5548(2018)03-0011-05

DOI:10.13732/j.issn.1008-5548.2018.03.003

收稿日期:2018-01-30, 修回日期:2018-03-28,在线出版时间:2018-05-08。

基金项目:西南科技大学研究生创新基金资助项目,编号:17ycx112。

第一作者简介:张明宇(1993—),男,硕士研究生,研究方向为除尘净化与干燥。E-mail:434864653@qq.com。

通信作者简介:陈海焱(1964—),男,博士,教授,研究方向为超细气流粉碎技术。E-mail:chenhai-yan@163.com。