ISSN 1008-5548

CN 37-1316/TU

Journal Online  2017 Vol.23
<Go BackNo.3

Preparation of high-activated aluminum powder by ball milling method

WANG Lulu1 , DENG Guodong1 , YIN Qiushi1 , HE Narenchaogetu1 , LI Duo2 , LI Qiag2

(1. National Special Superfine Powder Engineering Center, Nanjing University of Science and Technology, Nanjing 210094, China; 2. Shanxi North Xing'an Chemical Industry Company, Taiyuan 030008, China)

Abstract:To improve the aluminized explosive detonation heat performance, explore preparation method of high-activated aluminum powder, spherical aluminum powders were processed with a ball mill, and the effects of agitation speed, grinding time and grinding aid ratio on particle size, morphology and thermal properties of activated aluminum powder were studied. The morphology, particle size, and thermal decomposition of activated aluminum powder were characterized by scanning electron microscopy, laser particle size tester and synchronous thermal analyzer. Active aluminum content was determined by thermal analysis parameter method. Experimental results show that the best conditions to prepare active aluminum powder are stirring speed of 1 100 r/min, grinding time of 4 h, grinding aid ratio of4%. Under these conditions, the particle size d50 of the aluminum powder after grinding is 1.108 μm, and the active aluminum content of active aluminum powder is increased from 90.42% to98.42%. In aluminized explosive, detonation heat value is increased from 6 805 to 7 642 kJ/kg.

Keywords: spherical aluminum powder; content of active aluminum; ball milling; detonation heat; thermal decomposition performance

中图分类号:TQ56-0        文献标志码:A

文章编号:1008-5548(2017)03-0034-05

DOI:10.13732/j.issn.1008-5548.2017.03.007

收稿日期:2017-03-15, 修回日期:2017-03-22,在线出版时间:2017-06-28。

基金项目:国防火炸药科研专项项目,编号:AS03141。

第一作者简介:王路路(1990—),男,硕士研究生,研究方向为含能材料的研究。E-mail:847268139@qq.com。

通信作者简介:邓国栋(1965—),男,高级工程师,硕士生导师,研究方向为含能材料工艺研究。E-mail:13505196092@163.com。