ISSN 1008-5548

CN 37-1316/TU

Journal Online  2017 Vol.23
<Go BackNo.3

Research progress on preparation of graphene by liquid exfoliation method

TIAN Jie, GUO Li, SHEN Song, ZHANG Yi, YIN Xianglu, WU Wei

(High Gravity Engineering Research Center of Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, China)

Abstract:The selection principle of the graphite stripping system, the graphene stripping systems including the organic solvent system, the aqueous surfactant system and the ionic liquid system, and the stripping equipments such as the ball mill, the high pressure jet machine, the ultrasonic generator, the high speed mixing shear, the supercritical device and the high-gravity rotating bed were reviewed. It is considered that the method of liquid-phase exfoliation is the most promising preparation method because of its low cost, simplicity, high yield and latent industrial expansibility. There are many shortcomings, such as low concentration, the polydispersity of layer and size, expensive or high boil of stripping medium, difficult separation of auxiliary agent. The major challenge in preparing graphene is the selection and design of suitable stripping system and equipment.

Keywords: graphene;liquid-exfoliation;system;equipment

中图分类号:TQ 127.1+1          文献标志码:A

文章编号:1008-5548(2017)03-0045-05

DOI:10.13732/j.issn.1008-5548.2017.03.009

收稿日期:2016-10-22, 修回日期:2017-01-11,在线出版时间:2017-06-28。

基金项目:国家自然科学基金项目,编号 :21376025,21676023。

第一作者简介:田杰(1992—),女,硕士研究生,研究方向为纳米材料。E-mail:646300529@qq.com。

通信作者简介:毋伟(1966—),男,教授,博士生导师,研究方向为微纳米粉体制备及应用。E-mail:wuwei@mail.buct.edu.cn。