WU Fufeia , DONG Shuangkuaib , GONG Jingweia , SHI Kebina , LIU Sihaia
(a. College of Civil and Hydraulic Engineering; b. College of Pratacultural and Environmental Sciences, Xinjiang Agricultural University, Urümqi 830052, China)
Abstract:To investigate the distribution of lithium slag particle size, the effect of mass concentration of lithium slag solution, ultrasonic dispersion time and frequency, and dispersion medium on particle size of lithium slag was analyzed by a LS-POP (Ⅵ) type laser particle size analyzer. The correlation of specific surface area measured by a SBT-127 type digital Blaine permeability surface area analyzer and a laser particle size analyzer was discussed. The results show that comparing with kerosene and anhydrous ethanol, the dispersion effect of lithium slag is better by water which is suitable for a dispersion medium to lithium slag. Taking water as the dispersion medium, the test conditions of lithium slag particle size are as follows. The mass concentration of lithium slag solution is 3 to 4 g/L,ultrasonic dispersion time is not less than 4 min, and dispersion frequency is not less than 40 k Hz. Repeating the experiment five times with these conditions, it is found that distribution curves coincide of lithium slag particle size is relatively good, and the coefficient of variation of median diameter is less than 3%. The correlation between specific surface areas measured by the methods of laser diffraction and digital Blaine permeability is good, but the former is less than the latter.
Keywords: lithium slag; particle size; detection condition; correlation
文章编号:1008-5548(2016)01-0083-04
DOI:10.13732/j.issn.1008-5548.2016.01.020
收稿日期:2015-04-26, 修回日期:2015-05-10,在线出版时间:2016-02-22。
基金项目:高等学校博士学科点专项科研基金项目,编号:20106504110005;新疆维吾尔自治区研究生科研创新项目,编号:XJGRI2014072;新疆水利水电工程重点学科基金项目,编号:XJzdxk-2010-02-12。
第一作者简介:吴福飞(1985—),男,博士研究生,研究方向为水工混凝土耐久性。 E-mail:392429521@qq.com。
通信作者简介:侍克斌(1957—),男,博士,教授,博士生导师,研究方向为水利工程。 E-mail:xndsg@sina.com。