WANG Hongtaoa, b , CHEN Xiaoa, b , BAI Xiaobob , SONG Jieguanga , JI Gangchanga , DONG Zengxiangb
(a. School of Mechanical and Materials Engineering; b. Jiujiang Key Laboratory for Green Remanufacturing, Jiujiang University, Jiujiang 332005, China)
Abstract: High-performance ultrafine SiC powders were prepared by the method of ball milling taking low grade coarse SiC powders as raw materials. Effect of ball milling parameters such as milling time, mass ratio of ball to powders and rotation velocity on the microstructure and properties of SiC powders was researched. The results show that particle size and vibration compaction density of the SiC powders decrease with the increase of milling time, mass ratio of ball to powders and rotation velocity. However, taper height of the SiC powders increases, namely flowability of the SiC powders becomes poor. X ray diffraction peaks intensity decreases and full-widths at the half maximum (FWHM) of SiC diffraction peaks obviously broadens, which illustrates that grain sizes of the SiC powders are refined by ball milling. The optimal ball milling parameters are as follows. The rotation velocity is 200 r/min, the mass ratio of ball to powders is 10 and the milling time is 40 h.
Keywords: ball milling; SiC powder; microstructure
文章编号:1008-5548(2015)05-0009-06
DOI:10.13732/j.issn.1008-5548.2015.05.002
收稿日期:2014-10-27,修回日期:2014-12-04,在线出版时间:2015-10-21。
基金项目:国家自然科学基金项目,编号:51001056;江西省高等学校科技落地计划项目,编号:KJLD12096;江西省自然科学基金项目,编号:20151BAB206008;江西省教育厅科技项目,编号:GJJ13721;江西省“十二五”重点学科“材料加工工程”。
第一作者简介:王洪涛(1975—),男,博士,副教授,研究方向为机械合金化技术、金属基复合材料。 E-mail:wanght7610@163.com。
通信作者简介:纪岗昌(1961—),男,博士,教授,研究方向为材料表面强化与涂层技术。 E-mail:jgc@jju.edu.cn。