(Department of Dyeing and Chemistry, Shandong Silk Textile Vocational College, Zibo 255300, China)
Abstract: Taking zinc nitrate hexahydrate as zinc sources, ZnO nano-spheres constituted by the oriented aggregation of nano-particles were synthesized by hydrothermal method. ZnO spheres with various diameters were obtained by regulating volume ratios of triethanolamine to H2O. The structure and morphology of the obtained samples were characterized by XRD, IR, SEM and UV -Vis. The results show that the samples are hexagonal wurtzite ZnO. The possible growth mechanism of the nano-spheres is that ZnO nano-crystalline particles are synthesized from zinc nitrate hydrolyzed in triethanolamine solution and then directionally aggregated.
Keywords: ZnO nano-sphere; hydrothermal method; optical absorption; growth mechanism
中图分类号:TB383,TQ132·4+1 文献标志码:A
文章编号:1008-5548(2014)02-0064-04
DOI:10.13732/j.issn.1008-5548.2014.02.015
收稿日期:2013-06-08, 修回日期:2013-07-04,在线出版时间:2014-05-04。
基金项目:山东省高等学校优秀青年教师国内访问学者项目,编号:鲁教人函[2007]11。
第一作者简介:郭春芳(1977—),女,硕士,讲师,研究方向为功能材料制备与应用。 E-mail:guochunfang77@126.com。