ISSN 1008-5548

CN 37-1316/TU

Journal Online  2013 Vol.19
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Synthesis of Ultrafine Copper Powders by Chemical Reduction Under Ultrasonic Field

HUANG Jinfang, LIAO Huiwei, LEI Huili, DAI Wen, ZHANG Junru

(School of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China)

Abstract:Ultrafine copper powders were prepared by chemical reduction under ultrasonic field, with triethanolamine complexes of copper as raw materials and aluminium powders as reducing agents. The phases, microstructure, inoxidizability and surface-coating feature of resultant copper powders were confirmed by XRD, SEM, FTIR and TG. The stability of the copper powders was measured based on the measurements of their resistance. The results indicate that the ultrafine copper powders obtained by using cetrimonium bromide as surfactant under ultrasonic field have better dispersibility and greater inoxidizability.

Keywords:ultrafine copper powder; triethanolamine complexes of copper; surfactant; inoxidizability

中图分类号:O614.121            文献标志码:A

文章编号:1008-5548(2013)05-0063-04

DOI:10.3969/j.issn.1008-5548.2013.05.013

收稿日期:2013-03-10,修回日期:2013-04-11,在线出版时间:2013-10-25。

基金项目:国家自然科学基金项目,编号:21201142。

第一作者简介:黄晋芳(1989—),女,硕士研究生,研究方向为低维纳米功能材料制备与应用。 E-mail: huangjinfang1989@163.com。

通信作者简介:廖辉伟(1967—),男,教授,研究方向为低维纳米功能材料及工业废弃物处置与资源化。 E-mail: liaohw6709@163.com。