ISSN 1008-5548

CN 37-1316/TU

Journal Online  2013 Vol.19
<Go BackNo.6

Effects of Gelatin on Ultra-fine Silver Powders Prepared by Liquid Phase Reduction Method

DENG Nanlin, YUAN Gecheng, LIU Hua, LUO Zhijie, LI Qian, QIN Diancheng

(School of Materials and Energy, Guangdong University of Technology, Guangzhou 510006, China)

Abstract:With ascorbic acid as reductant, gelatin as dispersant, AgNO3 as reaction precursor, ultra-fine sliver powders were prepared by liquid phase reduction method. The effects of dosage and adding ways of gelatin on particle size, morphology and dispersion were investigated, and the dispersion mechanism of gelatin was explored. The silver powders were characterized by means of XRD, EDS, SEM and TEM. The results show that the ultra-fine silver particles are nearly spherical, and 0.1 to 1.2 μm in size. There is no significant effect of gelatin on the morphology of silver particles, but some effects on the particle size and the dispersion. As the dosage of gelatin increase the size of silver particles is larger, the dispersion is better. The dispersion mechanism of gelatin is mainly stereohindrance effect.

Keywords:ultra-fine silver powder; gelatin; dispersion mechanism

中图分类号:TQ063          文献标志码:A

文章编号:1008-5548(2013)06-0041-04

DOI:10.3969/j.issn.1008-5548.2013.06.010

收稿日期:2013-03-28,修回日期:2013-04-25,在线出版时间:2013-12-25。

基金项目:广东省科技计划项目,编号:2006B14701003。

第一作者简介:邓南林(1988—),女,硕士研究生,研究方向为超细粉体的制备。 E-mail:dengnanlin@163.com。

通信作者简介:袁鸽成(1963—),男,教授,研究方向为先进轻金属及微粉材料。 E-mail:gchyuan@gdut.edu.cn。