摘 要:用共沉淀法在不同热处理工艺下制备纳米 ZrO2 粉 体。样品的 T EM、SAXS、BET 和 XRD 分析结果表明热处 理对纳米 ZrO2 粉体性能的影响是显著的。结合实验与理论 分析得出粉末颗粒长大、团聚的机制与热处理对成分、粒度 及微观结构变化的作用。
关键词:纳米 ZrO2 粉体;热处理;性能
Abstract:Series of nano-ZrO2powders were prepared under dif ferent technology of heat treatment.All the resultscome from T EMSAXABET and XRDindicated that the influence of heat treatment on the performance of nano-ZrO2 was notable. Combining the experimental results and theoretical analysisthe mechanism of particleʾs growth and aggregationand the effect of heat treatment upon the change of compositiongranularity and microstructure were obtained.
Keywords:nano-ZrO2powders;heat treatment;performance