ISSN 1008-5548

CN 37-1316/TU

2009年15卷  第1期
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纳米TiO2粉尘的湿法捕集与表征

Collection and Characterization of TiO2 Nano-aerosol by Wet Method

Doi:
作者:杨毅,王正萍,陈守文,周先国

摘要:结合泡沫吸收塔除尘原理和雾滴湍流冲击原理等多种粉尘捕集原理,自制一种新型纳米粉尘湿法捕集装置,可对空气中纳米粉尘进行有效采集。对装置的采集原理及各部件进行了深入分析和详细介绍。根据绘制的纳米TiO2吸光度与浓度的工作曲线,应用分光光度法测定捕集液中纳米TiO2粉尘的浓度,进而准确掌握被采集区域空气中纳米TiO2粉尘的浓度。分别用纳米粒度仪和电子显微镜对装置采集到的纳米TiO2粉尘与实际生产纳米TiO2产品进行表征,结果发现两者在粒度分布和形貌等方面均表现出很好的一致性。

关键词:纳米粉尘;捕集装置;湿法

Abstract:The foam capture theory of dust tower and onflow fogdrop im-paction principle were employed and combined to develop a sampling de-vice for nanometer aerosols.The nano-aerosols could be sampled effective-ly with the self-made device.The sampling mechanism and functions of its parts were introduced in detail.Based on the working curve of absorbency and concentration of nanometer TiO2,the concentration of TiO2 of sam-pling liquid in the sampling device could be tested with spectrophotometer at 410 nm wavelength.According to the result,the concentration of TiO2 nano-aerosol in the air was calculated precisely.The nanometer sizer and TEM were employed to test the diameter distributions and microstructure profiles of TiO2 of sampling and producing,respectively.The results pre-sented good consistency with each other.

Keywords:nano-aerosol;sampling device;wet method