ISSN 1008-5548

CN 37-1316/TU

2009年15卷  第5期
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氧化钇稳定氧化锆陶瓷酸性环境下低温时效性能

Low Temperature Aging Effects of Y2O3 Stabilized Tetragonal Zirconia Polycrystals Ceramics in Acidic Environment

Doi:10.3969/j.issn.1008-5548.2009.05.005
作者:谢启飞,王晨,董利民,昝青峰,田杰谟

摘要: 研究了 4 种氧化钇稳定氧化锆陶瓷在弱酸性环境下的低温时效 对力学性能的影响。 每种氧化钇稳定氧化锆陶瓷陶瓷材料均分为对照 组和时效组,时效组置于 80 ℃、质量分数为 4%的醋酸溶液中时效 168 h。 采用 X 射线衍射分析试片表面单斜相含量,测试试条的三点弯曲强 度,用电子显微镜观察试条断口形貌。 结果表明,低温时效后 4 种氧化 钇稳定氧化锆陶瓷陶瓷的表面单斜相含量有不同程度的增加, 但抗弯强度无显著变化。 

关键词: 氧化锆;酸性环境;低温时效

Abstract:The influence of low-temperature degradation (LTD) treatment on the mechanical properties of four kinds of Y2O3 stabilized tetragonal zir conia polycrystals (Y-TZP) ceramics in weak acidic environment was re searched. Every kind of Y-TZP ceramics was divided into two groups:the control group and the LTD group. The LTD groups were put in the 4% acetic acid at 80 ℃ for 168 h. XRD was used to determine the volume con tent of monoclinic phase. The three-point flexural strength of the speci mens was measured. Fracture surface of the specimen were evaluated by scanning electron microscopy (SEM). The results revealed that after LTD in weak acidic environment the content of monoclinic phase increased in different degrees in the surface of four Y-TZP ceramics,but the flexural strengths were not significantly changed.

Keywords:zirconia;acidic environment;low-temperature degradation