ISSN 1008-5548

CN 37-1316/TU

2013年19卷  第5期
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煅烧工艺对TiO2-白炭黑光催化材料性能的影响

Effect of Calcinations on Properties of TiO2-Precipitated SiO2 Photocatalysts

Doi:10.3969/j.issn.1008-5548.2013.05.016
作者:汪 滨, 郑水林, 桂经亚, 张广心

摘要:以白炭黑和TiCl4为原料, 利用低温水解沉淀方法在白炭黑载体表面负载纳米TiO2, 采用煅烧工艺将白炭黑负载的纳米TiO2复合粉体进行晶化, 并对煅烧后的复合粉体进行晶体结构和光催化性能的表征。结果表明, 700℃煅烧2 h得到的样品, 在200 W高压汞灯的照射下, 35 min时对罗丹明B的脱色率达到96.23%。

关键词:白炭黑;纳米TiO2;光催化

Abstract:Taking precipitated silica and TiCl4 as raw materials, a kind of coated nano-sized TiO2 composite photocatalysts was prepared by the means of hydrolysis-depositing method. The effect of calcination on crystal structure and photocatalytic activity of the composite photocatalysts was investigated. The results show that the decolorization rate of rhodamine B of the composite photocatalysts calcined at 700 ℃ for 2 h is 96.23% under the irradiation of 200 W Hg lamp for 35 min.

Keywords:precipitated silica; TiO2nano-particle; photocatalysis