ISSN 1008-5548

CN 37-1316/TU

2014年20卷  第5期
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表面活性剂辅助微波法合成氧化锌纳米粉体

Synthesis of Zinc Oxide Nano-particles by Surfactant Assisted Microwave Method

Doi:10.13732/j.issn.1008-5548.2014.05.014
作者:李海霞

摘要:研究表面活性剂对微波辐照反应条件下合成氧化锌晶体的结构、形貌和紫外吸收性的影响,采用透射电子显微镜、X射线衍射、能量散射X射线光谱和紫外-可见吸收光谱对样品进行分析表征。结果表明:改变表面活性剂的种类可以制备出棒状、带状和多孔结构的氧化锌晶体;合成的氧化锌均为单晶,具有较强的紫外吸收特性和可见光透过性。

关键词:氧化锌;微波辐照法;纳米带;纳米棒


Abstract: The effect of various surfactants on structure, morphology and UV-Vis properties of zinc oxide crystals prepared by microwave irradiation method were studied. TEM, XRD, EDAX and UV-Vis spectrum were used to analyze the structure and morphology of as-obtained samples. The results show that different morphologies such as rods, belts and particles of zinc oxide crystals can be obtained by changing types of surfactants. All as-obtained samples are single-crystal zinc oxide and have strong properties of ultraviolet absorption and visible light permeability. 

Keywords: zinc oxide; microwave irradiation; nano-belt; nano-rod