ISSN 1008-5548

CN 37-1316/TU

2016年22卷  第2期
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乙二胺四乙酸根插层镁-铝水滑石的制备与性能

Preparation and Performance of EDTA Intercalated Mg-Al Layered Double Hydroxide

Doi:10.13732/j.issn.1008-5548.2016.02.011
作者:衷水平,陈良哲,伍赠玲,陈鸿

摘要:通过共沉淀法合成乙二胺四乙酸根(EDTA4-)插层的镁-铝水滑石(MgAl-EDTA-LDH),并采用X射线衍射和红外光谱对其结构和化学组成进行表征,研究MgAl-EDTA-LDH对水溶液中铜离子的去除能力。结果表明,乙二胺四乙酸根已插入镁-铝水滑石的层间,且插层水滑石能有效吸附水溶液中的铜离子,在2 h时吸附效率可达93.05%。

关键词:重金属废水;插层;水滑石;铜离子

Abstract:The EDTA4- intercalated Mg-Al layered double hydroxide(MgAl-E DTA-LDH) was prepared by the method of co-precipitation.The structure and chemical compositions of Mg Al-EDTA-LDH were characterized by XRD and IR. The removal of copper ion in aqueous solution by MgAl-EDTA-LDH was researched. The results show that EDTA4- is intercalated into the interlayer spaces of Mg-Al layered double hydroxide.The Mg Al-EDTA-LDH can remove Cu2+ from the aqueous solution effectively with the maximum adsorption efficiency of 93.05% at 2 h.

Keywords: heavy metal waste water;intercalation;layered double hydroxide;copper ion